• 专利附录
  • 专利说明
  • 权利要求
  • 类似技术
  • 同族专利
  • 引用文献
  • 法律状态
  • 优先权
    • 专利摘要:
    Climate chamber for a rheometer with at least one opening for the passage of the measuring shaft of the rheometer and control of the prevailing temperature and humidity in the chamber via a flowing through the chamber climate medium with means for temperature control and moisture.
    公开号:AT513661A1
    申请号:T12472012
    申请日:2012-11-27
    公开日:2014-06-15
    发明作者:
    申请人:Anton Paar Gmbh；
    IPC主号:
    专利说明:

    27-Nov-2012 11:44 Anton Paar GmbH 0316257257 4/26 .SheoFK012012
    Climate chamber for a rheometer with humidity control and convection temperature control system with heat pumps
    The invention relates to a climate chamber for controlling and monitoring the environmental conditions (temperature and humidity) in a rheometer, in particular a rotational and / or extensometer, consisting of an upper Meeateil and a lower measuring part, which are movable relative to each other, and one between the two The climate chamber surrounds the measuring parts and the measuring gap at a distance and this climate chamber allows rheological measurements on material samples over a wide temperature and humidity range.
    Rotational rheometers are precise instruments for determining the rheological properties of viscoelastic samples. In the rotational rheometer, the samples (liquid or solid) in the measuring space between two measuring parts (which may have different geometries) are subjected to shear stress on measuring axes by rotation or oscillation of the two measuring parts relative to each other and the torque or forces occurring through the sample of shear are measured and determined in an evaluation unit, the rheological parameters of the sample.
    Depending on the experimental procedure, the rheological measured variables (shear rate and shear stress) are determined in an evaluation unit from the alternatively specified or measured raw data (rotational speed and torque). Such a 27/11/2012 11:49 2/24 wr. : R796 P, 004/026 27-Nov-2012 11.44 Anton Paar GmbH 0316257257 5/26 27-Nov-2012 11.44 Anton Paar GmbH 0316257257 5/26 2 .. * & & heoFK012012
    Rotationsrheometer is described for example in AT404 192 B. For the highest measuring accuracy in the rheometer, the exact determination of the speed of rotation of the drive and the torques caused by the shear load with virtually frictionless support of the drive and / or measuring shafts and an exact determination of the distance s between the two measuring parts (the stability of the
    Environmental conditions) of great importance. The shape of the measuring parts takes in each case on the sample to be examined and the measuring range under consideration consideration / in the art cylinder measuring systems / cone-plate »or plate-plate arrangements or special application-specific measurement combinations are known. Examples are, for example, the arrangement according to US 6 / 578,413, the stretch rheological measurements on fibers and films by means of counter-rotating drums at the measuring part enable position or the arrangement for dynamic mechanical thermal analysis (DMTA) of the applicant, the material characterization in torsion and elongation of rod-shaped Solid state samples are allowed by clamping in two opposing measuring jaws, or special cells allowing tribological measurements, such as the Applicant's arrangement shown in AT505938 (B1).
    In addition, however, also e.g. special extensometers are known, such as the extensometer shown in US 6,711,941 for determining the rheological properties of a sample by tensile tests by means of axial gap extension. The measuring parts are moved relative to each other in the axial direction. In this case, the upper measuring part is usually deflected axially with a motor or piston arrangement and the reaction of the sample is determined by measuring the tensile behavior, strain rates and / or optical observation of the deformation behavior. 27/11/2012 11:49 ru 2: 4 R796 P.005 / 026 27-Nov-2012 11:44 Anton Paar GmbH 0316257257 6/26 27-Nov-2012 11:44 Anton Paar GmbH 0316257257 6/26 • · «· ··· • · ♦ · *.! RheoFK012012
    In general, the sample to be examined is located in the rheometer in a defined measuring space or measuring gap between the two measuring parts, the two measuring parts are adjustable relative to one another and at least one of the two measuring parts is connected to a drive motor and / or measuring motor via a measuring shaft. The rheometer arrangement is located on a stand that holds the measuring parts in a defined position to each other.
    Since the viscoelastic samples to be examined generally exhibit strongly temperature-dependent behavior, the sample temperature plays a central role in these measurements, shear tests at a constant temperature are used in addition to defined heating and / or cooling rates. The minimization of a temperature drift during the measurement process, the prevention of temperature fluctuations and thus also fluctuations of the measuring gap height etc. are of great relevance for the accuracy of the measurement. The samples to be examined are therefore tempered, for example directly by means of heating elements in the measuring parts. In order to minimize the temperature drift caused by heat radiation, the measuring space is closed off by an insulated housing against the environment. The measuring space or measuring gap and the measuring parts of precision rheometers in the prior art are therefore generally surrounded by a closed climate chamber, which allows a temperature control over wide temperature ranges.
    For example, Applicant's sample chamber / tempering chamber, which has been on the market since 2000 under the name CTD 600, makes it possible to temper the sample chamber with electrical heating in the chamber wall and at the same time to flow it through with a suitable inert gas, around the sample, the measuring parts and the sample space to temper by the combination of convection and heat radiation. Temperatures 27/11/2012 11:50 4/24 hrs: R796 P.006 / 026 27-Nov-2012 11:44 Anton Paar GmbH 0316257257 7/26 • * • # * • · · · * • · · · ·: RheoFK0120l2 under the prevailing ambient temperature is achieved by flowing through the sample chamber by means of suitable coolants (liquefied gases, for example liquid nitrogen) and, in combination with the electric heater in the measuring chamber wall, to the desired temperature. However, this procedure has the disadvantage that complex and expensive LPG cooling is necessary. For many standard measurements, for example on polymers, the width of the coverable temperature range does not make sense. Therefore, in addition to electrical Heizanordnugen also chambers with Peltiertemperierung exist. Such a sample chamber is described, for example, in AT 409 422 B.
    Especially in the investigation of the rheological properties of polymers, the moisture content of the samples also plays a major role. Investigations on samples with different moisture content are desirable to investigate the relationship between moisture and rheological properties. As a rule, the samples are prepared in a climate chamber and then measured in the rheometer. Controlled environmental conditions around the measuring gap are necessary in order to avoid problems during the measurement by drying out the samples, on the other hand it is also desirable to directly determine the change of the rheological properties on a sample (in situ) and to vary the moisture content of the samples. Optionally, the experimental setup should also be optically e.g. be monitored by camera.
    The expansion rheometer presented in US Pat. No. 6,711,941 has, according to the description, a closed chamber in which, in addition to the temperature control of the sample by supplying tempered gas and temperature control system, the achievement of a specific relative humidity by means of supply 11/50/2012 11:50 n / P.007 / 026 27-Νον · 2012 11:44 Anton Paar GmbH 0316257257 8/26 5 .. · '• RheoFK0120l2 humid gas into the sample chamber or by evaporation of liquid in the chamber is possible.
    However, the shown simple supply and temperature control of the system hinders the constant of the sample temperature, which is indispensable for the measurements in precise rotational rheometers, without temperature drift at sample and measuring parts as well as the optimal optical monitoring of the experiments by formation of condensates on the chamber windows.
    The invention thus relates to a climate chamber for cost-effective temperature control of material samples in a rheometer in the temperature range of about - 20 ° C up to 200 ° C to counteract the problems known in the art condensation and temperature drift.
    In this case, the system should be heated and / or cooled in this temperature range by means of a heat pump / Peltier elements and without supply of expensive LPG / refrigerant and the need for a second temperature control for the cooling gas for measurements under the room temperature available.
    The measuring accuracy of the rotational and / or extensional rheometer is increased by largely avoiding temperature drift in the sample and the measuring points.
    Furthermore, due to the tempering of the measuring chamber wall surrounding the measuring chamber and an optionally included in this viewing window condensation on the windows should be prevented.
    The samples can be optically monitored and optical measurements taken through windows in the 27/1 1/2012 1 1:50 ru 24 R796 P.008 / 026 27-Nov-2012 11.44 Anton Paar GmbH 0316257257 9/266 .. * • · · · ··· · · · ♦ * .iRheoPK012012
    Chamber wall without obstructions by condensation of the supplied moisture to the optical measuring instruments are performed.
    In the following the invention with reference to the embodiments according to the drawings will be explained in more detail.
    1 shows an embodiment according to the invention of the climatic chamber 10 on a double motor rheometer. The two Rheometermessteile 1.2 (here in plate-plate geometry upper plate 1 and lower plate 2) form the measuring gap or measuring space S, in which the sample to be measured is 3. The measuring shafts (5) on the upper (5a) and lower (5b) measuring part lead either to measuring motors or to the drive motor of the rotary rheometer; this can be a double-rotor system according to AT 508.706 or a rotary rheometer with separate drive and measuring motor. Optionally, this shaft can be used a motor for linear movement of a measuring part parallel to the direction measuring shaft to realize a linear expansion rheometer, (indicated by moving arrows) The term measuring shaft is used mutatis mutandis extensively for measuring and drive shafts of rheometers.
    The rheometer generally consists of two interconnected units. The rheometer head 6a and rheometer base 6b contain the respective motors and / or measuring systems of the rheometer, which are not described in more detail here. The connection of the two rheometer units, for example via a stand 7 offers the possibility to adjust the distance between the measuring parts in the axial direction. The entire test procedure is controlled software-supported with the evaluation and display unit 8 and carried out the different measurement methods. 27/11/2012 11:51 7/24 No .: R796 P.009 / 026 27 · Νον-2012 11:44 Anton Paar GmbH 0316257257 10/26 •• RheoFK0120l2
    The climate chamber 10 is installed in the space between the rheometer base 6b and the measuring head of the rheometer 6a on the stand 7. The interior 4 of the climate chamber 10 surrounds the measuring parts 1 and 2, the measuring gap with the sample 3 and the inner parts of the measuring shafts 5 and 5a. The housing is insulated from the outside world by suitable insulation material (for example suitable materials such as styrofoam, insulating foam or the like or arrangements with insulating air chambers, vacuum, etc.), but has additional openings 11a and 11b in order to carry out the measuring shafts of the measuring parts can. Thus, the measuring waves 5a, 5b of a rotary and / or Dehnheometers record without additional friction losses acting through the sample under load forces.
    The climate chamber may contain additional openings along with suitable optically transparent covers to allow in situ optical observations of the sample under strain / shear and / or strain load. It is important to ensure a good thermal connection of the transparent portions of the climate chamber.
    The climate chamber is dimensioned so that different measuring part geometries and different measuring room designs can be used. (Cup systems, cone plate and plate plate systems of different diameters, strainers with corresponding holders, etc.)
    To facilitate the exchange of measuring parts and the entry of samples, the housing is easy to open b2w. arranged in several parts and displaceable.
    Preferably, the housing is mounted in two parts on a rail system 17a and / or 17b in order to be able to connect the housing to the rail 27a and 11b / 26 - * RheoFK0l2012
    Move housing radially or axially apart and open and slide when closing again in the desired position / lock.
    Alternatively, headband can be used and the MesBkammerteile swung out of their experimental position. Alternatively, the climate chamber can be made removable.
    The housing wall is designed in a layered structure and optionally assembled by means of mating elements such as pins and / or locking quick-release fasteners and / or connectors.
    In the walls of the climatic chamber 10, which delimits the interior 4 of the climate chamber are at least partially housed heat pumps to temper the heat-conducting inner wall of the chamber. In this case, the inner wall of the chamber is expediently designed completely or partially as a heat exchanger.
    As an environmental medium, a possibly pre-tempered carrier gas (air or other gaseous medium suitable for conducting experiments, for example inert gas) is subjected to the corresponding moisture by means of a moisture generator 20 and fed into the inlet or inlets 22 of the climatic chamber. The humidity generator is connected via a hose system 21 or directly to the climate chamber. The climate media transport preferably takes place via a flexible heated hose. The climate medium is fed via a connection 22 in the climate chamber. The climate medium in the climate chamber and / or climatic chamber wall is directed to the openings 11a and 11b. The transport preferably takes place through the heat exchangers of the climatic chamber walls in order to increase the climate medium to the temperature of the chamber wall. 27/11/2012 11:51 9/24 Nr .: R796 P.011 / 026 27-Nov-2012 11:44 Anton Paar GmbH 0316257257 12/26 • ·· · 5, iheoFK0120l2 bring. Thus, a further temperature control of the climate medium is not absolutely necessary.
    Outlets 12 for the Xlimamedium are attached to the openings 11a and 11b for the passage of the measuring waves, the measuring medium surrounds the measuring waves perpendicularly or directed into the climatic chamber at an angle α * 0 to 90 degrees, in particular at an angle of 20 to 70 degrees , preferably 45 degrees,
    The climate medium flows around the measuring shaft in the area of the climatic chamber, the measuring parts and the measuring gap resp. Measuring chamber and is passed through the at least one outflow opening 14 in the climatic chamber wall from the climatic chamber. Preferably, the entire climate chamber is under slight overpressure relative to the ambient pressure. Preferably, the outlet is at the height of the measuring parts. Alternative arrangements with, for example, an arrangement with guide channels in the chamber wall or openings in the bottom of the climatic chamber are possible.
    As a result of this overpressure, climate medium flows out of the climate chamber in the area of the contactless transmission of the measuring waves and can thus cause condensation on the measuring waves. On the one hand, the condensate can enter the sensitive rheometer heads or flow back into the climate chamber. A tempering of the measuring waves and thus increased temperature conduction of the measuring waves in the rheometer can be done. Therefore, in addition to the described guidance of the climate medium, a second, preferably dry, gaseous medium or ambient air is used for thermal insulation and moisture decoupling of the rheometer components. Via supply line 24 & and an inlet 24 in the climatic chamber wall, this gas is directed to the openings 11a and 11b and over the 27/11/2012 11:52 10/24 "in the r .: R796 P.012 / 026 27-Νον · 2012 11:44 Anton Paar GmbH 0316257257 13/26 ···························································································································································································································································· the measuring shaft directed Ausläese 13 directed against the measuring shaft.
    At least one of the measuring waves is thereby directed vertically and / or out of the climate chamber outward. The outflow angle β may be in a range of 0 to 90 degrees, in particular 20 to 70 degrees, preferably 45 degrees in the direction of the measuring parts.
    With such an arrangement, temperature ranges of approximately -20 ° C. to 180 ° C. (dry air) and / or at variable humidities of up to 95% relative humidity at 80 ° C. can be achieved in the climate chamber without influencing the measurements in the precision rheometer.
    2 shows a schematic diagram of the measuring chamber according to the invention on a precision rheometer with a tripod with its control and regulating circuits and supply and discharge lines. Optionally, the Peltier blocks used can also be equipped with countercooling. Cooling surfaces with connected water cooling are used for temperature control of the blocks.
    The climatic chamber 10 is arranged around the measuring shafts 5a and 5b openly between the rheometer head 6a and rheometer 6b and encloses the measuring parts and sample. The control and evaluation of the rheometer or a separate control and regulation unit for the climatic chamber 8 is connected to the humidity generator 20 and the controller for the cooling circuit 27.
    The cooling circuit is connected via inlet and outlet 27a and inlet or outlet 27b with the climate chamber. The temperature control of the Peltier elements in the climatic chamber walls takes place via the connection line 28 27/11/2012 11:52 11/24 nr ,: R796 P.013 / 026 27-Nov * 2Q12 11:44 Anton Paar GmbH 0316257257 14 / 26 ·· 11 · · · · · · · 99 »9 9 9 9 9 9 9 9 9 9 9 99 99 * · • · * · • I · .. • .iRheoFK012012
    A moisture measuring element 15 is mounted in the region of the air conditioning outlet 14, which together with a temperature measuring element 18 on the climate chamber wall supplies the control parameters for the generation of temperature and humidity.
    In addition, a connection 24 is provided for the supply of dry gas. Here, by way of example, a gas cylinder 24b is connected to nitrogen via connecting line 24a into the channels of the climatic chamber, but the supply line can also be made via the gas connections in the laboratory (dry air or the like). The temperature of this purge gas is preferably at the ambient temperature. With this gas guide the motors and measuring and control elements of the rheometer are shielded from the atmosphere of the climatic chamber. The heating of the motors by heat conduction over the measuring waves and condensation of moisture from the climate medium at the measuring waves is prevented.
    In general, such climate chambers are equipped with a door to access the climate chamber interior and to change sample and measurement parts.
    In order to make the measuring system usable in a wide variety of experimental arrangements and to ensure the modularity of the rheometer arrangement (a measuring system from simple plate / plate tests to tensile tests (eg SER) and tribology measurements), the measuring chamber wall is preferably made in two parts and can be mounted centrally a rail system 28 for measuring part - and sample change open or be swung apart.
    FIG. 3 shows in detail the structure of the layer structure climatic chamber wall. The inside P.014 / 026 12/24 27/11/2012 11:53 no .: R796 27-Nov-2012 11:44 Anton Paar GmbH 0316257257 15/26 ·· ······· · 12 έϋβώκοΐ2οΐ2 the Wall 10 a is formed from the surface of a heat exchanger 31. In the preferred embodiment, the heat exchanger forms the entire inner wall of the measuring chamber. The material used for the heat exchanger is of good thermal conductivity and chemically resistant to the samples and gases tested in the rheometer. Optionally, when measuring chemically aggressive samples, the measuring chamber inner wall can be coated with an inert material. The heat exchanger is crossed by at least one, preferably a plurality of interconnected channels 32. These channels are located in the volume of the heat exchanger, they can be performed several times in a suitable form (eg. In meandering or spiral shape) in the material of the heat exchanger. By having the largest possible surface area, it is achieved that no additional tempering device is required for the supplied gas, the conditioned medium supplied is guided through the heat exchanger over as wide a surface as possible and thus tempered to the temperature of the heat exchanger or the sample chamber inner wall.
    The heat exchanger is connected at the side facing away from the chamber interior 4 with at least one, but preferably a plurality of heat pumps 33. These heat pumps can be mounted in the walls enclosing the measuring parts and / or in the bottom and / or in the upper part of the climate chamber with the feedthroughs for the measuring shaft. With this heat pump (s), preferably Peltier blocks, the temperature of the heat exchanger and thus the heat radiation in the measuring chamber is controlled. At the same time, the gas flowing into the measuring chamber can thus be tempered.
    On the outside of the side facing away from the interior 4 of the climate chamber side of the Peltier elements is optionally a counter-cooling with heat exchangers 35, traversed by the fluid 27:11 12:53 13/24 ιί r .: R796 P.015 / 026 27-Nov-2012 11:44 Anton Paar GmbH 0316257257 16/26 13
    ** Cooling medium (air, water or a special cooling fluid) via connection 36 and outflow 37.
    As is known in the prior art, the heat exchanger can be designed block-shaped, possibly with passages or with cooling fins.
    The entire assembly is sealed against the environment by means of suitable insulating materials 38. On the outside of the chamber are located in this material, the feeds for the drying gas, which flows around the measuring shafts 5a and / or 5b outwardly directed.
    This results in a uniform and cost-effective tempering (both heating and cooling) of the measuring chamber by the Peltier elements.
    In the measuring chamber 4 uniform flow patterns arise, as indicated by the arrows 9, which minimize the temperature drift in the sample 3.
    The chamber contains viewing windows in the half-shells in order, for example, to be able to carry out optical measurements on the samples under shear stress or to be able to mount a CCD camera on the outside, for example for extension rheological examinations.
    The viewing windows may be mounted opposite each other for optical measurements in either half-shell or may be attached to the sample as a larger window to use a CCD camera. Practically, the dimensions of the window sections are chosen so, 27/11/2012 11:53 14/24 Dir .: R796 P. 016/026 27-Nov-2012 11:44 Anton Paar GmbH 0316257257 17/26 27-Nov-2012 11 : 44 Anton Paar GmbH 0316257257 17/26 14 • 9 I · • 9 · 99 9 · • · · · · · · · · · · · · · · · · · · · · · · · · · ·········································
    RhebBK0l2012 that different measurements with one and the same chamber are possible.
    4 shows an alternative embodiment of a rheometer with a combined measuring and drive motor, which both drives a measuring part (1) and measures the acting torques. Here, the measuring part (2) without measuring shaft is simply attached to the RheometerfuS 6b. Optionally, this measuring part (2) can be tempered separately by arrangements in Rheometerfuß6b. The climate chamber is placed as a hood on the Rheometerfuß and here has only one passage opening 11 for the measuring shaft (5). The flushing of the measuring shaft with air medium via inlets 12 and dry purge gas with outlets 13 is analogous to the version with 2 measuring shafts. Connection 22 for the climate medium and inlet 24 for the dry gas lead into the climate chamber, the discharge opening 14 is preferably in the height of the measuring part. The open entire climate chamber can be done here for example via a holding and displacement device 17c in the vertical direction. The chamber can also have a door to make the measuring chamber interior accessible. 27/11/2012 11:54 15/24 in the r. : R796 P.017 / 026
    权利要求:
    Claims (13)
    [1]
    27-Νον · 2012 11:44 Anton Paar GmbH 0316257257 18/26 15

    1. Climate chamber for a rheometer, in particular rotational and / or Dehnrheometer consisting of two measuring parts (1,2), which act on a material sample to be examined by a movement of the measuring parts relative to each other with a defined shear and / or Dehnbelastung and from the measurement of the resulting flow and / or deformation behavior of the sample in a connected evaluation unit determines its rheological parameters, the measuring chamber comprises the measuring space on all sides and tempered by a combination of convection and heat radiation, characterized in that the wall surrounding the sample space Climate chamber contains at least one opening which is suitable for non-contact implementation of Messteilachse or Messteilachsen through the walls of the climatic chamber and the sample space is flowed through by a tempered fluid Klimamedium, preferably air, preset temperature and humidity ,
    [2]
    2. Climate chamber according to claim 1, characterized in that the introduction of the environmental medium via inlets 12 in the region of the implementation 11 / lla, llb of at least one measuring parts or the measuring parts through the climatic chamber wall and the at least one measuring shaft directed perpendicular or in the climatic chamber lapped, wherein the inflow angle o in a range of 0 to so degrees, in particular 20 to 70 degrees, 27/11/2012 11:54 16/24 No .: R796 P.018 / 026
    [3]
    27-Nov-20l2 11:44 Anton Paar GmbH 0316257257 19/26
    [4]
    27-Nov-20l2 11:44 Anton Paar GmbH 0316257257 19/26 16 ••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••• towards the measuring parts. 3. Climate chamber according to one of the preceding claims, characterized in that the inner walls of the climate chamber are constructed of thermally conductive material which is heated by heating elements and / or a heat pump
    [5]
    4. Climate chamber according to one of the preceding claims, characterized in that the gas flowing into the chamber is tempered before entering the climate chamber by means of flow channels in the thermally conductive material of the climatic chamber and the open chamber flows through a temperature whose amount is less than or equal to the temperature amount of Inner walls of the chamber and / or the heat exchanger is.
    [6]
    5. Climate chamber according to claim 5, characterized in that the heat pump consists of at least one Peltier element with additional countercooling, and thus the introduced climatic chamber medium to temperatures between - 40 0 C and 200 ° C is heated.
    [7]
    6. Climate chamber according to one of the preceding claims, characterized in that additional outflow openings for another gaseous, preferably dry medium are attached to the at least one implementation of the measuring wave for the upper and / or lower measuring part of the rheometer and the measuring waves evenly with the gaseous medium P.019 / 026 17/24 27/11 / 2012 1 1:54 iu.: R796
    [8]
    27-Nov-2012 11:44 Anton Paar GmbH 0316257257 20/26
    [9]
    17-Nov-2012 11:44 Anton Paar GmbH Rtia & iK012012 flow outward perpendicularly or out of the climatic chamber, the outflow angle β being directed between 0 and 90 degrees against the measuring shaft, in particular the angle β is between 20 and 70 degrees, preferably at 45 degrees. 7. Climate chamber according to one of the preceding claims, which contains on its inner wall and / or the interior of the climatic chamber and / or the discharge opening for the climate medium, a measuring element for measuring the humidity and / or the temperature of the air flowing through the chamber climate medium, and with the measured values, the supply and / or temperature control of the climate medium controls. 8. Climate chamber according to one of the preceding claims, wherein the supply of the environmental medium is carried out of a humidity generator.
    [10]
    9. Climate chamber according to claim 7, characterized in that the temperature of the climate medium is regulated on the basis of the measured humidity and / or temperature of the climate medium on the temperature of the heat pump and optionally the countercooling by the evaluation unit
    [11]
    10. A method for determining the rheological properties of viscoelastic samples, which are subjected to a stretching and / or shearing between two measuring parts of a rheometer, under defined climatic conditions in a surrounding the measuring parts and the measuring chamber climatic chamber, P.020 / 026 18/24 27/11/2012 11:55 wr .: R796
    [12]
    27-Nov-2012 11:44 Anton Paar GmbH 0316257257 21/26
    [13]
    27-Nov-2012 11:44 Anton Paar GmbH 0316257257 21/26 18 RftefcSK0120l2 characterized by the fact that the partially open climatic chamber is flowed through by a climate medium of defined humidity and temperature and due to the guidance of the climate medium in the climatic chamber a symmetrical flow around the Results in measuring parts, so that the measured values of the rheometer are not influenced by the air medium flowing through. 11. The method according to claim io, characterized in that the at least one measuring shaft of the measuring part / the measuring parts of the rheometer is flushed during the flushing of the climatic chamber with the gaseous medium through additional channels and openings with a second dry fluid medium outside the climatic chamber and thus the thermal Load on the measuring motor (s) and the formation of moisture on the measuring shaft (s) is prevented. 27/11/2012 11:55 19/24 No .: R796 P.021 / 026
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    引用文献:
    公开号 | 申请日 | 公开日 | 申请人 | 专利标题
    DE10058399A1|1999-11-29|2001-05-31|Anton Paar Gmbh Graz|Rotation rheometer, has heat pump, especially Peltier block, provided to heat, cool or temperature regulate upper measurement part with gap to lower measurement part|
    DE10147200A1|2001-09-25|2003-04-10|Thermo Haake Gmbh|Rotational|
    DE10350554A1|2003-10-29|2005-06-02|Thermo Electron Gmbh|Rotary- or extension rheometer for e.g. foods or paints, includes additional sensor unit for measurement and control of humidity and pressure in measurement chamber|
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    AT516382B1|2015-03-13|2016-05-15|Anton Paar Gmbh|Conditioning a sample container by means of conditioning fluid for promoting heat coupling and suppressing fogging|
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    法律状态:
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    申请号 | 申请日 | 专利标题
    AT12472012A|AT513661B1|2012-11-27|2012-11-27|rheometer|AT12472012A| AT513661B1|2012-11-27|2012-11-27|rheometer|
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